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Catalytic Hydrocracking of a Bitumen‐Derived Asphaltene over NiMo/γ‐Al2O3 at Various Temperatures 下载免费PDF全文
Hydrocracking of a bitumen‐derived asphaltene over NiMo/γ‐Al2O3 was investigated in a microbatch reactor at varying temperatures. The molar kinetics of asphaltene cracking reaction was examined by fitting the experimental data. Below a defined temperature, the molar reaction showed the first‐order kinetic feature while at higher temperatures secondary reactions such as coke formation became significant, causing deviation of the reaction behavior from the proposed first‐order kinetic model. Selectivity analysis proved that dominant products varied from gases to liquids to gases with increasing temperature, shifting the dominant reaction from C–S bonds cleavage to C–C bonds cleavage. 相似文献
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Sumeng Wei Yuling Yang Xiao Feng Shanshan Li Lei Zhou Jingyu Wang Xiaozhi Tang 《International Journal of Food Science & Technology》2020,55(7):2691-2699
Structures and properties of myofibrillar protein gel prepared at different power (300–800 W) were evaluated. Amino acid analysis demonstrated that changes in microwave power did not alter primary structure of gel. However, an increase in microwave power could change higher structures of gel. As microwave power increased, α-helix content decreased and β-sheet content increased. Increased microwave power probably facilitated protein to unfold and expose the internal groups, causing surface hydrophobicity and the formation of disulphide bonds were enhanced, which indicated changes in tertiary and quaternary structures of protein. At 500 W, gel had the best ultrastructure where surface morphology, springiness and water holding capacity reached the optimum. Our findings suggested that microwave at an appropriate power (500 W) could change higher structures of myofibrillar protein gel to achieve desired processing and quality protein gel characteristics. 相似文献
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Fei Li Xin-Gang Wang Xiao Huang Ji-Xuan Liu Weichao Bao Guo-Jun Zhang Hongzhi Wang 《Journal of the European Ceramic Society》2018,38(14):4806-4813
We present a straightforward method via sol-gel process using polyethylene glycol (PEG) as phase separation inducer to prepare zirconium carbide/silicon carbide (ZrC/SiC) porous monoliths. Organic/inorganic hybrid gels are prepared using zirconium oxychloride, furfuryl alcohol, and tetraethyl orthosilicate as major starting materials. In the presence of PEG, crack-free hybrid monoliths are obtained by drying the wet gels under ambient pressure, whereas in the absence of PEG, the wet gels break into pieces as expected. PEG plays a key role in maintaining the macroscopic shape of the monoliths. After ceramization at 1300–1500?°C, ZrC/SiC porous monoliths are obtained. SEM and mercury intrusion porosimetry data show that PEG also has strong influence on the microstructures of the monoliths. The compressive strengths of the ceramic monoliths are in the range of 0.3 to 0.7?MPa. And their compressive behavior starts to differ due to the changes in their microstructures, especially the pore structure. 相似文献
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通过硬度测试、拉伸性能测试、透射电镜观察等分析手段研究了不同强变形工艺下2519A铝合金的力学性能与微观组织。结果表明,经50%的冷轧变形和165 ℃人工时效后,2519A合金的力学性能明显提高,其抗拉强度、屈服强度和伸长率分别为522 MPa、468 MPa和8.5%。而在冷变形前添加165 ℃×2 h预时效处理,合金的力学性能进一步提高,其抗拉强度、屈服强度和伸长率分别达到535 MPa、497 MPa和8%。预时效处理可以提高合金中θ′相的密度,使析出相分布更加均匀,有助于提高合金的力学性能。 相似文献
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采用普通涤纶、含1%云母颗粒的涤纶(1%云母/涤纶)以及含5%云母颗粒的涤纶(5%云母/涤纶)三种材质,上机纬密采用200根/10 cm、300根/10 cm、400根/10 cm,组织采用平纹、斜纹、缎纹试织试样。通过Hot Disk热常数分析仪,采用正交试验及极差、方差分析,研究了纤维材质、上机纬密、组织对凉感纤维织物导热系数的影响。结果表明:在试验设置变量范围内,纤维材质对导热系数的影响显著,上机纬密、组织对导热系数的影响高度显著,影响因素从大到小顺序为上机纬密>组织>纤维材质。 相似文献